[Al7{N(SiMe3)2}6]−: A First Step towards Aluminum Metal Formation by Disproportionation

Abstract
A “naked” aluminum atom links two aluminum tetrahedra in the [Al7{N(SiMe3)2}6] ion (see picture), which results from the reaction of a metastable AlCl solution with LiN(SiMe3)2 and crystallizes with [Li(OEt2)3]+ as cation. This unique structure among molecular metal atom clusters represents a small but characteristic section of cubic close-packed aluminum.

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