Metallaoxetene formation by coupling of carbamoyl and difluorocarbene ligands

Abstract
The reaction of the carbamoyl complex [Fe{C(O)NPri 2}CF3(CO)2(PPh3)] with potassium hydrotris(pyrazo-1-yl)borate provides the structurally characterized ferraoxetene[Fe{CF2OC(NPri 2)}(CO){HB(pz)3}](pzpyrazol-1-yl), presumably via coupling of the carrbamoyl of the carbammoyl ligand with a difluorocarbene intermediate.

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