Notizen: Convenient Preparation and Vibrational Spectra of Cyclodecasulfur, S10, and of the Adduct S6 · S10 [1]
Open Access
- 1 October 1978
- journal article
- research article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 33 (10) , 1198-1200
- https://doi.org/10.1515/znb-1978-1032
Abstract
Thermal decomposition of S6O2 and S7O, respectively, in CH2Cl2 or CS2 solution at temperatures between 20 and 5 °C yields SO2, polymeric sulfur and S10 which was obtained as pure single crystals in yields of 7-11% with regard to the starting materials S6 and S7, respectively. Infrared and Raman spectra of S10 as well as of the new molecular addition compound S6 · S10 are reported.Keywords
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