Reactions of 1,2-dichlorohexafluorocyclopentene with secondary phosphines
- 1 August 1968
- journal article
- Published by Canadian Science Publishing in Canadian Journal of Chemistry
- Vol. 46 (15) , 2625-2628
- https://doi.org/10.1139/v68-428
Abstract
Dicyclohexylphosphine and diphenylphosphine react with 1,2-dichlorohexafluorocyclopentene to give almost exclusively the monoderivative via displacement of a vinylic chlorine atom. With the former phosphine a disubstituted derivative is also found. In addition to analytical values and infrared spectroscopic data, both 19F and 31P nuclear magnetic resonance spectra support the proposed structures.Keywords
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