Characterization of pentacarbonylvanadate(–III) and hydridopentacarbonylvnadate(–II) by13C,15V, and1H n.m.r. spectroscopy
- 1 January 1984
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 14,p. 893-894
- https://doi.org/10.1039/c39840000893
Abstract
N.m.r. spectra of highly reduced vanadium carbonyls containing 99% enriched 13CO in liquid ammonia at –50 °C provide the first direct spectroscopic evidence for the existence of Na3[V(CO)5] and Na2[HV(CO)5] in solution.Keywords
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