One-Step Synthesis of 9-Oxodecanoic Acid and its Methyl Ester; A Useful Starting Material for Prostaglandin Synthesis
- 1 January 1980
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1980 (09) , 751-753
- https://doi.org/10.1055/s-1980-29201
Abstract
The title acid was prepd. from cyclohexanone. Cyclohexanone was treated with H2O2 in HClO4, water was added, and the org. phase was sepd. and added to TiCl3, CH2:CHCOMe, and Me2CO at room temp. to give 9-oxodecanoic acid. Similarly, 10-oxoundecanoic acid was prepd. from cycloheptanonKeywords
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