Hydrogen bonding in organic synthesis. Part 6. C-Alkylation of β-dicarbonyl compounds using tetra-alkylammonium fluorides
- 1 January 1977
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 1
- No. 15,p. 1743-1745
- https://doi.org/10.1039/p19770001743
Abstract
Mono-C-alkylation of a number of β-dicarbonyl compounds using alkyl iodides and tetra-alkylammonium fluorides is described. Yields are high with primary iodides and isopropyl iodide, but much lower with s-butyl and t-butyl iodides. The reactions occur under mild conditions with no apparent O-alkylation or other competing reactions.Keywords
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