Absolute configuration of (+)-2-exo-bromonorbornane 1-carboxylic acid and (–)-1-iodo-2-exo-bromonorbornane
- 1 January 1986
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 4,p. 297-299
- https://doi.org/10.1039/c39860000297
Abstract
Resolution of (±)-2-exo-bromonorbornane-1-carboxylic acid was achieved by h.p.l.c. separation of diastereoisomeric amides, obtained from this acid and (+)-(R)-phenylglycinol; the absolute configuration was established by X-ray structure analysis and correlated with c.d. spectra.Keywords
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