In situ synthesis of phenyltrithiophosphonate: isolation and structure of [PPh4]2[W2S4{S2(S)PPh}2]

Abstract
PhP(S)S2 2– has been prepared directly by the reaction of [PPh4]2[WS4] with PhPCl2; [PPh4]2[W2S4{S2(S)PPh}2] has been isolated and the anion shown to involve a W2S4 core to which are ligated two bidentate PhP(S)S2 moieties.

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