Phosphorus-Fluorine Chemistry, XXXI
Open Access
- 1 August 1972
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 27 (8) , 879-884
- https://doi.org/10.1515/znb-1972-0802
Abstract
The preparation of a series of methyl-substituted piperidyl-fluorophosphoranes is described, of general formula RR′NPF4-nPhn (where RR′N = 2-Me-piperidyl-, 3-Me-piperidyl-, or 4-Me-piperi-dyl; n = 0, 1, or 2), from the cleavage of silicon-nitrogen bonds in methyl-substituted piperidyl silanes by fluorophosphoranes. The structures of the new compounds are deduced from 19F and 31P n.m.r. data.Keywords
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