Co-condensation of molybdenum atoms with the bulky tertiary diphosphine 1,2-bis(di-isopropylphosphino)ethane: the molecular structure of [MoH4(Pri 2PCH2CH2PPri 2)2]

Abstract
Co-condensation of molybdenum atoms with the tertiary diphosphine 1,2-bis(di-isopropylphosphino)ethane affords the stereochemically non-rigid, eight-co-ordinate tetrahydride complex [MoH4(Pri 2PCH2CH2PPri 2)2]. The crystal structure has been determined in the orthorhombic space group Ccca(no. 68), with cell parameters a= 18.351(2), b= 20.164(2), c= 9.150(6)Å, and Z= 4.

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