Eight-co-ordinated zirconium(IV) Schiff-base compounds: an X-ray study

Abstract
The crystal structure of tetrakis-(N-ethylsalicylaldiminato)zirconium(IV) contains eight-co-ordinated (dodecahedral) tetrachelated zirconium in the unusual S4 configuration with remarkably long Zr–N bond lengths; n.m.r. evidence suggests that the N-isopropyl derivative is also eight-co-ordinate whereas the N-t-butyl derivative involves a lower co-ordination of the zirconium.

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