Optimization of Sample Preparation Techniques for the Determination of 4-Nonylphenol in Water and Sediment
- 1 January 1996
- journal article
- research article
- Published by Taylor & Francis in Journal of Liquid Chromatography & Related Technologies
- Vol. 19 (2) , 259-275
- https://doi.org/10.1080/10826079608005511
Abstract
Sample preparation techniques for the determination of 4-nonylphenol in water and sediments were optimized using two-level orthogonal array design (OAD). Comparison between the use of cartridge-based solid-phase extraction and membranous disk-based extraction was made for water samples. For sediment samples, microwave-assisted solvent extraction (MASE) was employed. A comparison between MASE and classical soxhlet extraction of spiked samples was also carried out. 4-Nonylphenol was determined using high performance liquid chromatography (HPLC) coupled to both ultraviolet and fluorescence detectionKeywords
This publication has 22 references indexed in Scilit:
- Orthogonal array designs for the optimization of liquid chromatographic analysis of pesticidesAnalytica Chimica Acta, 1994
- Development and application of a multi-residue analytical method for the determination of n-alkanes, linear alkylbenzenes, polynuclear aromatic hydrocarbons and 4-nonylphenol in digested sewage sludgesWater Research, 1994
- The effects of nonylphenol on Daphnia magnaWater Research, 1993
- p-Nonyl-phenol: an estrogenic xenobiotic released from "modified" polystyrene.Environmental Health Perspectives, 1991
- Bioaccumulation of 4-nonylphenol in marine animals— A re-evaluationEnvironmental Pollution, 1990
- Lethal and sublethal toxicity of 4-nonylphenol to the common mussel (Mytilus edulis L.)Environmental Pollution, 1989
- Occurrence and behaviour of linear alkylbenzenesulphonates, nonylphenol, nonylphenol mono- and nonylphenol diethoxylates in sewage and sewage sludge treatmentWater Research, 1988
- Simultaneous determination of linear alkylbenzene sulfonates, alkylphenol polyethoxylates, and nonylphenol by high-performance liquid chromatographyAnalytical Chemistry, 1987
- Microwave-extraction -a new method superseding traditional Soxhlet extractionZeitschrift für Lebensmittel-Untersuchung und Forschung, 1987
- Persistent organic chemicals in sewage effluents. 2. Quantitative determinations of nonylphenols and nonylphenol ethoxylates by glass capillary gas chromatographyEnvironmental Science & Technology, 1982