A novel type of photosubstitution of [fac-Re(bpy)(CO)3Br](bpy = 2,2′-bipyridine) with P(OR)3in the presence of triethylamine: efficient formation of [Re(bpy)(CO)2{P(OR)3}2]+Br

Abstract
Photochemical ligand substitution of [fac-Re(bpy)(CO)3Br] with P(OEt)3 in the presence of triethylamine quantitatively gave [Re(bpy)(CO)2{P(OEt)3}3]+Br without the intervention of a mono-substituted product.

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