Abstract
The anionic pentasulphide chain S5 2– acts as a bidentate ligand to form the “hetero-cyclohexahalcogen”(C5H5)2TiS5: the TiS5 ring fragment has the chair conformation with Ti–S bond lengths of 2·420 and 2·446 Å and S–S bond lengths which range from 2·051–2·059 Å.

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