New NHR Techniques for Structure Determination and Resonance Assignments of Complex Carbohydrates
- 1 January 1984
- journal article
- research article
- Published by Taylor & Francis in Journal of Carbohydrate Chemistry
- Vol. 3 (4) , 593-611
- https://doi.org/10.1080/07328308408057920
Abstract
This paper describes several new NMR techniques for structure determination and spectral assignment of polysaccharides. Positions of linkages between sugar units can be determined unambigously and with high sensitivity using a modified version of the well known INEPT experiment. A new two-dimensional experiment is shown to provide excellent resolution and sensitivity in correlating 1H and 13C chemical shifts.This publication has 22 references indexed in Scilit:
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