Abstract
The configurations and preferred conformations of a number of perhydro-oxazolo[3,4-c]oxazines and perhydro[1,3]oxazino[3,4-c][1,3]oxazines have been assigned on the basis of their n.m.r. spectra. The conformational preferences of these compounds have been interpreted in terms of the minimisation of dipolar type interactions arising from the 1,3 arrangements of the heteroatoms.

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