Separation of Aldoses and Alditols Using Thermostable Open Tubular Glass Capillary Columns
- 1 June 1973
- journal article
- separations
- Published by Taylor & Francis in Analytical Letters
- Vol. 6 (6) , 479-493
- https://doi.org/10.1080/00032717308058696
Abstract
Successful GLC separation of complex mixtures of aldoses and alditols has been achieved. Aldoses are analyzed as the poly-O-acetylaldonic nitriles (Wohl derivatives), and polyols are analyzed as the polyacetyl esters. When mixtures of aldoses and alditols are subjected to the conditions of the Wohl synthesis, each component forms a single derivative. Terminal dissymmetry is retained for aldoses. Analyses are made using 60 m SE-30 open tubular glass capillary columns with temperature programming.Keywords
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