Synthesis of 1,2-bis(1,4,7,10-tetra-azadodecanyl)ethane, a double-ring fully saturated macrocycle containing 12-membered tetra-aza subunits

Abstract
The title compound, a fully saturated bimacrocycle (1), has been obtained through a procedure involving the protection of all but one of the amino nitrogen atoms of each tetra-aza ring which are then bridged by an ethylenic segment; (1) behaves as a dinucleating ligand, forming a dicopper(II) complex in which there is a weak ferromagnetic interaction between the metal atoms.

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