Non-planar structures of Et3N and Pri3N: a contradiction between the X-ray, and NMR and electron diffraction data for Pri3N
- 1 January 1998
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 7,p. 781-782
- https://doi.org/10.1039/a708399h
Abstract
The crystal structures of Et3N and Pri 3N were determined by X-ray analysis using the in situ crystallization technique for single crystal growth on the diffractometer; both have a pyramidal configuration of the nitrogen atom, even Pri 3N, which was considered to be planar in accord with electron diffraction and NMR data.Keywords
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