Abstract
Fluorine nuclear magnetic resonance (F‐NMR) has been used to determine dissociation constants for multipolar complexes formed by several p‐substituted fluorobenzenes in CCl4 and cyclohexane at 25°. Data in CCl4 were also obtained at −20°. The results are interpreted in simplified terms as dipole‐dipole interactions which lead to a complex of net zero dipole moment. Although the dissociation constants are not of high accuracy, the values obtained do indicate that both polarity and steric effects are important in the presumed multipolar complexes.