Total synthesis of (+)-validamycin B
- 1 January 1987
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 24,p. 1843-1844
- https://doi.org/10.1039/c39870001843
Abstract
The first complete synthesis of the antibiotic validamycin B as its dodeca-O-acetate is reported; coupling of the epoxide (6) and the partially protected valienamine derivative (14), followed by deprotection, gives the product (1b) which was identified by 1H n.m.r. spectroscopy.Keywords
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