An Efficient One-Pot Synthesis of 1,2-Benzenedithiol from Benzenethiol
- 1 January 1992
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1992 (05) , 451-452
- https://doi.org/10.1055/s-1992-26132
Abstract
1,2-Benzenedithiol (3) can be prepared on a molar scale and isolated in 96% yield by a convenient one-pot procedure starting from benzenethiol. This method utilizes recent discoveries on the formation of dilithium 1,2-benzenedithiolate (2) via directed ortho-lithiation of lithium benzenethiolate.Keywords
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