Abstract
Dimethyl(phenylchalcogeno)bismuthanes of the general formula (CH3)2BiEC6H5(E = S, Se, Te), the first m olecules with a Bi -Se or a Bi-Te-bond, respectively, were synthesized in good yields by reactions of tetramethyldibismuthane and diphenyldichalcogenides. At room temperature - these thermolabile compounds react quantitatively - with increasing rate in the series S-Se-Te to give CH3Bi(EC6H5)2 and Bi(CH3)3.

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