Mg/PbBr2Bimetal Redox-Promoted Stannation of Propargyl, Allyl, Vinyl, and Aryl Halides

Abstract
Reductive coupling of propargylic bromides with tributylstannyl chloride was performed in a regioselective manner by the aid of magnesium metal and a catalytic amount of lead(II) bromide in THF, affording allenyltributylstannanes. In a similar manner, allyl-, vinyl-, and aryl-tributylstannanes were prepared from the corresponding halides.

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