X-Ray crystal structure of 1,3,8,10-tetraoxacyclotetradecane
- 1 January 1972
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Perkin Transactions 2
- No. 12,p. 1726-1729
- https://doi.org/10.1039/p29720001726
Abstract
The molecular and crystal structure of the title compound has been determined from X-ray diffractometer data. The structure was solved by Patterson and Fourier methods and refined by least-squares techniques to R 0·058 for 775 independent reflections. Crystals are monoclinic, space group P21/n, with Z= 2 in a unit cell of dimensions: a= 8·107(3), b= 14·721(6), c= 4·724(1)Å, β= 100·25(8)°. The ring structure resembles that of cyclotetradecane as derived from the diamond lattice.Keywords
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