Chemie polyfunktioneller Liganden, 56 [1]. Darstellung von N-Deutero-bis(diphenylphosphino)amin, sowie schwingungsspektroskopischer Vergleich mit Bis(diphenylphosphino)amin und Lithium-bis(diphenylphosphino)amid / Chemistry of Polyfunctional Ligands, 56 [1]. Preparation of N-Deutero-bis(diphenylphosphino)amine, as well as the Vibrational Spectroscopic Comparison with Bis(diphenylphosphino)amine and Lithium-bis(diphenylphosphino)amid
Open Access
- 1 January 1980
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 35 (1) , 64-67
- https://doi.org/10.1515/znb-1980-0115
Abstract
Bis(diphenylphosphino)amine, [(C6H5)P2NH (1), can be metallated with n-butyl-lithium to hthium-bis(diphenylphosphino)amid, [(C6H5)P2NLi (2), It reacts with CH3OD to give N-Deutero-bis(diphenylphosphino)amine, [(C6H5)P2ND (3). The compounds were characterized by infrared, Raman, 1H and 31P NMR spectroscopy.Keywords
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