An Expedient Synthesis of Diethyl 1-Azidoalkylphosphonates via the Mitsunobu Reaction
- 1 January 1992
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1992 (04) , 367-368
- https://doi.org/10.1055/s-1992-26111
Abstract
Diethyl 1-azidoalkylphosphonates were obtained in high yield, and under mild conditions by the reaction of diethyl 1-hydroxyalkyl-phosphonates with hydrazoic acid in the presence of triphenylphosphine/diethyl azodicarboxylate (the Mitsunobu reaction).Keywords
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