EPITOPE MAPPING OF FUNCTIONAL DOMAINS OF HUMAN FACTOR VA WITH HUMAN AND MURINE MONOCLONAL-ANTIBODIES - EVIDENCE FOR THE INTERACTION OF HEAVY-CHAIN WITH FACTOR XA AND CALCIUM
- 1 July 1987
- journal article
- research article
- Vol. 70 (1) , 139-146
Abstract
We have purified a unique neutralizing IgG1, .kappa. monoclonal antibody (MAb) against factor V (F-V) from a patient''s plasma. This MAb (H2) demonstrated specificity for human F-V heavy chain (D), mol wt 105,000. Using an enzyme-linked immunosorbent assay (ELISA) we assessed the competitive binding to F-Va of H2, H1 (human MAb directed to light chain, F1F2), and two murine MAbs, B38 (to F1F2) and B10 (to activation peptide C1). All four antibodies are of high affinity with KD varying from 0.17 to 1.17 .times. 10-10 mol/L. They recognized distinct epitopes in F-V. F-Xa competed in a concentration-dependent fashion for binding of H1, H2, and B38 but not B10 to F-V/Va in the absence of phospholipids or platelets. Thus both F1F2 and D polypeptides of F-Va but not C1 interacted with F-Xa. All MAbs bound to F-V/Va in the absence of Ca++. However, free Ca++ (0.1 to 4.0 mmol/L) increased the amount of H1 and H2 bound to factor V/Va, 1.65-fold and 3.65-fold, respectively but had little effect on the binding of either murine MAbs. Prothrombin (20 .mu.g/mL to 400 .mu.g/mL) in the absence of phospholipid did not inhibit the binding of MAbs. These studies provide evidence for the first time for a direct interaction between human F-Va heavy chain and F-Xa and Ca++ and for the direct binding of F-Xa to F-Va in the absence of phospholipids or platelets and enhance our understanding of functional F-V domains.This publication has 25 references indexed in Scilit:
- Thrombin-catalyzed activation of human coagulation factor V.Journal of Biological Chemistry, 1982
- Studies of the capacity of factor Xa to protect factor Va from inactivation by activated protein C.Journal of Biological Chemistry, 1982
- Coordinate binding of factor Va and factor Xa to the unstimulated platelet.Journal of Biological Chemistry, 1981
- (p-Amidinophenyl)methanesulfonyl fluoride, an irreversible inhibitor of serine proteasesBiochemistry, 1980
- A rapid method for removal of [125I]iodide following iodination of protein solutionsAnalytical Biochemistry, 1980
- The calcium-binding properties of bovine factor V.Journal of Biological Chemistry, 1980
- The inhibition of blood coagulation by activated protein C through the selective inactivation of activated factor VBiochimica et Biophysica Acta (BBA) - Enzymology, 1979
- pH gradient elution of human IgG1, IgG2 and IgG4 from protein A-SepharoseJournal of Immunological Methods, 1979
- The subunit structure of thrombin-activated factor V. Isolation of activated factor V, separation of subunits, and reconstitution of biological activity.Journal of Biological Chemistry, 1979
- Hemorrhagic death associated with a high titer factor V inhibitorAmerican Journal of Hematology, 1978