Metal–oxo cluster-supported transition metal complexes: hydrothermal synthesis and characterization of [{M(phen)2}2(Mo8O26)] (M = Ni or Co)

Abstract
Two new metal–oxo supported transition metal complexes, [{M(phen)2}2(Mo8O26) (M = Ni or Co; phen = 1,10-phenanthroline) are synthesized by a hydrothermal method and characterized by X-ray crystallography, showing that the octamolybdate possesses a novel unprecedented structure and that [M(phen)2]2+ units are covalently bonded to the [Mo8O26]4– cluster.

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