Synthesis and characterization of a novel microporous aluminophosphate AlPO4-JDF (2AlPO4·HOCH2CH2NH2) from alcohol systems
- 1 January 1996
- journal article
- Published by Royal Society of Chemistry (RSC) in Journal of Materials Chemistry
- Vol. 6 (7) , 1207-1210
- https://doi.org/10.1039/jm9960601207
Abstract
The synthesis of a novel aluminophosphate microporous compound A1PO4-JDF (where J means Jilin University and DF is Davy Faraday Laboratory) containing organic amine in the presence of the template HOCH2CH2NH2 from predominantly non-aqueous media is described. Chemical and elemental analyses disclosed its idealized formula as 2A1PO4·HOCH2CH2NH2. A1PO4-JDF has been characterized by X-ray powder diffraction (XRD), IR spectroscopy, scanning electron microscopy (SEM), differential thermal analysis (DTA) and thermogravimetry (TG), and magic angle spinning nuclear magnetic resonance (MAS NMR) spectroscopy.Keywords
This publication has 14 references indexed in Scilit:
- Synthesis of AlPO4-17 from non-aqueous systemsJournal of the Chemical Society, Chemical Communications, 1994
- Silicoaluminophosphate with encapsulated methylbutylamine species: chabazite structure, charge coupling between framework and inferred ammonium species, and severe molecular disorderThe Journal of Physical Chemistry, 1989
- Synthesis and structure of a novel aluminoarsenate with an open frameworkJournal of the Chemical Society, Chemical Communications, 1989
- A molecular sieve with eighteen-membered ringsNature, 1988
- Crystal structures of the hydro-sodalite Na6[AlSiO4]6 8H2O and of the anhydrous sodalite Na6[AlSiO4]6Zeolites, 1986
- Aluminophosphate molecular sieves and the periodic tablePublished by Walter de Gruyter GmbH ,1986
- Silicoaluminophosphate molecular sieves: another new class of microporous crystalline inorganic solidsJournal of the American Chemical Society, 1984
- Location of cations in synthetic zeolites X and Y. Part 4.—Exchange limiting factors for Ca2+ in zeolite YJournal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1976
- A neutron-diffraction study of the crystal structure of analcime, NaAlSi2O6· H2OZeitschrift für Kristallographie, 1972
- Reinvestigation of the crystal structure of the zeolite hydrated NaXThe Journal of Physical Chemistry, 1970