Citrobacter lipopolysaccharides: structure elucidation of the O-specific polysaccharide from strain PCM 1487 by mass spectrometry, one-dimensional and two-dimensional 1H-NMR spectroscopy and methylation analysis
- 1 February 1985
- journal article
- research article
- Published by Wiley in European Journal of Biochemistry
- Vol. 146 (3) , 641-647
- https://doi.org/10.1111/j.1432-1033.1985.tb08699.x
Abstract
Structural studies on the O-specific polysaccharide of Citrobacter PCM 1487 lipopolysaccharide, using methylation analysis. Smooth degradation and 1H-NMR spectroscopy, indicate that it consists of the trisaccharide repeating units .**GRAPHIC**. In this structure, 4-deoxy-D-araHex stands for 4-deoxy-D-arabino-hexose.This publication has 17 references indexed in Scilit:
- Structural and Serological Analysis of Citrobacter‐036‐Specific Polvsaccharide, the Homopolymer of (βl→ 2)‐Linked 4‐Deoxy‐d‐arabinohexopyranosyl UnitsEuropean Journal of Biochemistry, 1981
- Improvement of 2D NOE and 2D correlated spectra by symmetrizationJournal of Magnetic Resonance (1969), 1981
- Structural analysis of glycosphingolipids by high-resolution proton nuclear magnetic resonance spectroscopyBiochemistry, 1980
- Studies of individual amino acid residues of the decapeptide tyrocidine A by proton double-resonance difference spectroscopy in the correlation modeBiochemistry, 1975
- Determination of aminosugar linkages in glycolipids by methylationArchives of Biochemistry and Biophysics, 1973
- Immunochemical Studies on Citrobacter O Antigens (Lipopolysaccharides)European Journal of Biochemistry, 1971
- Quantitative Determination of Monosaccharides as Their Alditol Acetates by Gas Liquid Chromatography.Analytical Chemistry, 1965
- The quantitative determination of galactose—An enzymic method using galactose oxidase, with applications to blood and other biological fluidsAnalytical Biochemistry, 1965
- Estimation of 3-Deoxy Sugars by Means of the Malonaldehyde–Thiobarbituric Acid ReactionNature, 1960
- [21] Preparation and analysis of d-glucosamine-6-phosphatePublished by Elsevier ,1957