Abstract
The kinetics and the mechanism of a reversible, intramolecular conversion of a coordinated nitrosyl ligand into a probably O,N-coordinated hydroxylamido(1-) ligand is reported for the complex anion [V(tha)(NO)(H2O)]- (tha = 1,1′,1″-nitrilo-tris-2-propanol). Mechanisms for the formation of nitrosyl complexes of the type {V-N=O}4 generated from hydroxylamine and complexes of vanadium in the oxidation states + V or + III, respectively, are proposed.

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