Organic Electronic Conductors and Precursors;1Reaction of Hexasodium Benzene-hexathiolate and Benzenehexathiol with Carbon Disulfide
- 1 January 1990
- journal article
- research article
- Published by Georg Thieme Verlag KG in Synthesis
- Vol. 1990 (12) , 1149-1151
- https://doi.org/10.1055/s-1990-27120
Abstract
The reaction of hexasodium benzenehexathiolate (1) and benzenehexathiol (7) with carbon disulfide is studied. Depending on the reaction conditions and the molar ratio of 1 or 7 to carbon disulfide the 1,3-benzodithiole-2-thiones 6, the 2,6-dithioxobenzo[1,2-d: 4,5-d′]- 5, the 2,5-dithioxobenzo[1,2-d: 3,4-d′]bis[1,3]dithiole 9 or the 2,5,8-trithioxobenzotris[1,3]dithiole (2) are obtained.Keywords
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