A New Microwave Reactor Suitable for Organic Synthesis and Kinetics Studies.1

Abstract
A microwave unit and reaction vessel for chemical synthesis or kinetics studies is described. The Teflon reaction vessel could be operated at temperatures up to 200°C and pressures up to 10 atmospheres. It was possible to stir and directly monitor the temperature and pressure in the microwave environment. The system was demonstrated by preparing isopropyl 2,4,6-trimethylbenzoate.

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