13C CP/MAS nuclear magnetic resonance of crystalline methylxylopyranosides
- 1 January 1985
- journal article
- Published by Canadian Science Publishing in Canadian Journal of Chemistry
- Vol. 63 (1) , 270-273
- https://doi.org/10.1139/v85-044
Abstract
The 13C nmr spectra of solids, acquired using the Cross Polarization/Magic Angle Spinning (CP/MAS) technique, are very sensitive to the detailed nature of crystalline packing. These effects are illustrated in the CP/MAS spectra of the α and β anomers of methyl-D-xylopyranoside. In the spectrum of the α anomer, which crystallizes with two molecules per unit cell, individual spectra can be resolved for the two molecules in the asymmetric unit of this crystal.Keywords
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