Synthese und Kristallstruktur von W2[OC(CF3)2NMe2]2(NMe2)4 / Synthesis and Crystal Structure of W2[OC(CF3)2NMe2]2(NMe2)4
Open Access
- 1 December 1986
- journal article
- Published by Walter de Gruyter GmbH in Zeitschrift für Naturforschung B
- Vol. 41 (12) , 1506-1508
- https://doi.org/10.1515/znb-1986-1205
Abstract
The reaction of W2(NMe2)6 with hexafluoroacetone (HFA) yields W2[OC(CF3)2NMe2]2(NMe2)4, an orange solid, which was characterized by mass spectra, 1H, 13C, 19F NMR spectra and an X-ray structure analysis. The compound contains a W=W triple bond of 230.1(1) pm.Keywords
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