Characterization of a Melpar Flame Photometric-Gas Chromatographic System for Application to Boron Hydrides
- 1 October 1971
- journal article
- Published by Oxford University Press (OUP) in Journal of Chromatographic Science
- Vol. 9 (10) , 632-634
- https://doi.org/10.1093/chromsci/9.10.632
Abstract
Decaborane (B10H14) has been used to characterize a Melpar Flame Photometric-Gas Chromatographic system as a sensitive and specific boron hydride detection system. Flame emission at 546 nm was used to define optimum oxygen, hydrogen, and air flow rates. A lower detection limit of 0.71 ng B10H14, as eluted from a 3% OV-1 Chromosorb W 80/100 mesh column, was obtained. Response is linear for greater than one order of magnitude from the lower limit of detectability.Keywords
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