Novel di-isopropylamino derivatives of trivalent phosphorus
- 1 January 1983
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 8,p. 477-478
- https://doi.org/10.1039/c39830000477
Abstract
Reduction of (Pri 2N)2PCl with LiAIH4 in diethyl ether gives (Pri 2N)2,PH; reaction of Pri 2NPCl2, with Mg in boiling tetrahydrofuran gives either the cyclotetraphosphine (Pri 2N)4P4 or the 1,2-dichlorobiphosphine Pri 2NP(Cl)–P(Cl)NPri 2 depending upon the Mg:Pri 2NPCl2 mole ratio.Keywords
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