Abstract
Rates and orientations of methoxydefluorination (NaOMe–MeOH) of twelve polyfluoronitrobenzenes have been measured at 298.2 K. The fluorine substituent effects are less well defined in the presence of the nitro-group, and are dependent not only upon the orientation of the fluorine substituent with respect to the reaction site, but also with respect to the nitro-group. The resulting attenuation seems to be electronic rather than steric in origin, and may be described as a mutually weakening interaction of the mesomeric effects of halogen and nitro-group. Two fluorine atoms ortho to the nitro-group cause a further diminution of effect consistent with this explanation.

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