Highlighting gyroscopic motion in crystals in 13C CPMAS spectra by specific isotopic substitution and restricted cross polarization
- 24 November 2004
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 2,p. 189-191
- https://doi.org/10.1039/b409744k
Abstract
The temperature-dependent exchange rate and signal coalescence in the 13C CPMAS NMR spectrum of a crystalline molecular gyroscope are exposed by specifically deuterating the overlapping static carbons.Keywords
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