Use of electrospray ionization mass spectrometry to characterize chiral reactive intermediates in a titanium alkoxide mediated sulfoxidation reaction
- 1 January 1997
- journal article
- Published by Royal Society of Chemistry (RSC) in Chemical Communications
- No. 9,p. 869-870
- https://doi.org/10.1039/a701227f
Abstract
The ESIMS technique, combined with 1 H NMR evidence, provides a precise inventory of the catalytic Ti IV precursors and the characterization of the reactive peroxometal complex involved in enantioselective sulfoxidation employing the Ti IV –homochiral trialkanolamine–alkylhydroperoxide system.Keywords
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