Efficient One-Pot Procedures for the Preparation of Secondary Phosphines
- 1 December 1994
- journal article
- research article
- Published by Taylor & Francis in Synthetic Communications
- Vol. 24 (22) , 3219-3223
- https://doi.org/10.1080/00397919408010243
Abstract
Secondary phosphines R2PH or RR'PH (R and R' = alkyl, cycloalkyl) have been obtained in good yields by preparing lithium phosphide from lithium, red phosphorus and t-butylalcohol in liquid ammonia and subsequent alkylation in the presence of alkali amide, prepared in the same flask.Keywords
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