Some Remarks on Obtaining of Very Pure P4S9
- 1 April 1994
- journal article
- research article
- Published by Taylor & Francis in Phosphorus, Sulfur, and Silicon and the Related Elements
- Vol. 89 (1-4) , 173-179
- https://doi.org/10.1080/10426509408020446
Abstract
Pure tetraphosphorus nonasulfide—form P4S9(I)—free of admixtures of other phosphorus sulfides was prepared in two steps. The first one was multistage extraction from the P—S melt containing only P4S9 and P4S7. The second was crystallization of the solid obtained in the first step.Keywords
This publication has 10 references indexed in Scilit:
- Über die Struktur einer neuen Modifikation des Phosphorsulfids P4S9Zeitschrift für anorganische und allgemeine Chemie, 1990
- Kinetic and mechanistic aspects of the redox dissociation of tetraphosphorus decasulphide in solutionJ. Chem. Soc., Dalton Trans., 1990
- A multiphase one- and two-dimensional 31P NMR investigation of P4S7Chemical Physics Letters, 1988
- 31P-KERNRESONANZUNTERSUCHUNGEN VON P4S9UND P4S10Phosphorus and Sulfur and the Related Elements, 1982
- BEMERKUNGEN ZUR DARSTELLUNG UND31P-KERNRESONANZ-UNTERSUCHUNGEN VON P4S5UND P4S7Phosphorus and Sulfur and the Related Elements, 1981
- 31 P NMR study of P4S7Chemical Physics Letters, 1981
- REDOX DISSOCIATION OF MELTED TETRAPHOSPHORUS DECASULFIDEPhosphorus and Sulfur and the Related Elements, 1981
- 31P NMR spectra of P4S9 and P4S10: comparison with related compoundsChemical Physics Letters, 1976
- Zur Kenntnis der neuen Phosphorsulfidphase P4S9. II. Über verschiedene Methoden zur Darstellung und über die Eigenschaften und Konstitution des P4S9Zeitschrift für anorganische und allgemeine Chemie, 1970
- Zur Kenntnis der neuen Phosphorsulfidphase P4S9. I. Über die Bildung von P4S9 bei der Hydrolyse von Phosphorthiochlorid im EinschlußrohrZeitschrift für anorganische und allgemeine Chemie, 1969