Synthesis of 24-methyl sterols stereospecifically labelled with 2H in the isopropyl methyl groups. 13C NMR spectral assignment of C-26 and C-27 resonances

Abstract
Through analysis of the 13C NMR spectra of (25S)-[27-2H]campesterol (1) and (25R)-[26-2H]dihydrobrassicasterol (2), the C-26 and C-27 resonances have been unambiguously assigned; the biosynthetic applications are discussed.

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