Generation and trapping of a phosphinine sulphide

Abstract
With sulphur at ca. 140 °C in xylene, 4,5-dimethyl-2-phenylphosphinine gives a transient P-sulphide which reacts with 2,3-dimethylbutadiene as a dienophile through its 1,6 positions and with dimethyl acetylenedicarboxylate as a diene through its 1,4 positions.

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