High resolution NMR in solids; A simple and improved ‘magic angle’ probe design for conventional small gap 13C FT spectrometers
- 1 June 1981
- journal article
- Published by Wiley in Magnetic Resonance in Chemistry
- Vol. 16 (2) , 85-89
- https://doi.org/10.1002/mrc.1270160204
Abstract
The mechanical and electronic design of a ‘magic angle’ NMR probe is described. This probe can be incorporated in a conventional small gap 13C FT spectrometer, without any hardware or software change, to obtain high resolution 13C NMR spectra on organic solids. A simple way of tuning the homogeneity and adjusting the angle is also proposed. Illustrative experimental results on various types of molecular crystals with different molecular mobilities, a clathrate compound and a polymer are discussed.Keywords
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