Iodine oxidation of unsaturated bunte salts
- 1 January 1972
- journal article
- research article
- Published by Royal Society of Chemistry (RSC) in Journal of the Chemical Society, Chemical Communications
- No. 17,p. 974-975
- https://doi.org/10.1039/c39720000974
Abstract
Oxidation of pent-4-enyl thiosulphate with iodine in refluxing water–ethanol yielded 2-ethoxymethyltetrahydrothiophen and 2-hydroxymethyltetrahydrothiophen instead of the expected pentenyl disulphide; treatment of pentenyl disulphide with iodine in refluxing water–ethanol produced the same products and the same percent yields as the oxidation of the 4-pentenyl-1-thiosulphate.Keywords
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