Zur Synthese der Hühnerinsulin-A-Kette, I. Darstellung der Fragmente A1–8, A9–15, A1–7 und A8–15

Abstract
By coupling the peptide derivatives H-Cys(SBut)-Cys(SBut)-His-OMe(6-8b) and H-Cys(SBut)-Cys(SBut)-OH(6-7b) respectively with Trt-Gly-Ile-Val-Glu(OBut)-Gln-OH(1-5a) the N-terminal sequences A1-8 and A1-7 of the chicken insulin A chain were prepared. The sequence A9-15 was obtained by connecting Bpoc-Asn-Thr(But)-Cys(SBut)-OH (9-11c) and H-Ser(But)-Leu-Tyr(But)-Gln-OH (12-15). Acylation of the aminopeptide derivative 9-15b with Bpoc-N2H3 yielded fragment A8-15(8-15).

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