A Facile Synthesis of α,α-Difluoroalkyl Ethers and Carbonyl Fluoride Acetals by Oxidative Desulfurization-Fluorination

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Abstract
α,α-Difluoro ethers and carbonyl fluoride acetals were readily prepared from thiocarboxylic O-acid esters and O, O′-disubstituted thiocarbonate, respectively, in moderate to good yields by the action of tetrabutylammonium dihydrogentrifluoride and N-bromosuccinimide or N-iodosuccinimide.

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